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A new method in synthesis of polyurethane/graphite oxide nanocomposites by twin-screw extruder

Van Thi Khanh Khuat 1, *
Tam Thanh Mai 1
Nhan Thuc Chi Ha 1
Huy Thuc Ha 1
  1. University of Science, VNU-HCM
Correspondence to: Van Thi Khanh Khuat, University of Science, VNU-HCM. Email: pvphuc@vnuhcm.edu.vn.
Volume & Issue: Vol. 16 No. 4 (2013) | Page No.: 45-53 | DOI: 10.32508/stdj.v16i4.1602
Published: 2013-12-31

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Copyright The Author(s) 2023. This article is published with open access by Vietnam National University, Ho Chi Minh city, Vietnam. This article is distributed under the terms of the Creative Commons Attribution License (CC-BY 4.0) which permits any use, distribution, and reproduction in any medium, provided the original author(s) and the source are credited. 

Abstract

In this study, we have synthesized polyurethane based on monoglyceride and 4.4 '-diphenyl methanediisocyanate (MDI) – an environmentally friendly polymer. Graphene oxite (GO) was used to reinforce for polyurethane forming polyurethane/graphene oxide (PU/GO) nanocomposite. The synthesis of PU and PU/GO was performed directly on the twinscrew extruder. This is a simple, time saving, economical and environmentally friendly method. Nanocomposites were manufactured with GO phase changed from 0.5% to 1.5% by weight. Structural analysis results of PU/GO showed a good dispersion through TEM figure (transmission electron microscopy). In addition, the mechanical and thermal properties of the nanocomposite were improved as compared to the original polyurethane. This study is a new step for the synthesis of polyurethane and nanocomposite based on polyurethane by the melt intercalation method.

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