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Synthesis of silver nano-particles using micro-emulsion technique

Hoa Phuoc Trung Nguyen 1
Tuyen Thuy Bich Pham 1
Vinh Quang Lam 1
Hieu Van Le 1
Volume & Issue: Vol. 16 No. 4 (2013) | Page No.: 75-84 | DOI: 10.32508/stdj.v16i4.1605
Published: 2013-12-31

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Copyright The Author(s) 2023. This article is published with open access by Vietnam National University, Ho Chi Minh city, Vietnam. This article is distributed under the terms of the Creative Commons Attribution License (CC-BY 4.0) which permits any use, distribution, and reproduction in any medium, provided the original author(s) and the source are credited. 

Abstract

Silver nanoparticles were synthesized by mixing two micro-emulsion systems – one with precursor (AgNO3) and one with reducing agent (NaBH4). Dioctyl sodium sulfonsuccinate – AOT was used as surfactant. We studied parameters as ω – molar ratio of water to surfactant, hydrocarbon (oil) types. The molar ratio of water to surfactant was changed from 2.5 to 5; 7.5 and 10. The used oil types were cyclohexane, iso-octane, and dodecane. XRD, UV-Vis and TEM images were used to elucidate the structure and size of the products. The results showed that, synthesized silver nanoparticles sizes were between 5 – 7 nm, with homogeneously spherical shapes. The silver colloids were used in antibacterial applications. The antibacterial efficiency was very high, above 99% at ~ 4 μg/ml concentration of silver nanoparticles.

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