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Reduction of graphene oxide by TiO2 nanotubes photocatalyst

Son Vinh Nguyen 1, *
Trinh Thi Diem Duong 1
Phuong Tuyet Nguyen 1
Nhu Thi So Le 1
  1. University of Science, VNU-HCM
Correspondence to: Son Vinh Nguyen, University of Science, VNU-HCM. Email: pvphuc@vnuhcm.edu.vn.
Volume & Issue: Vol. 18 No. 2 (2015) | Page No.: 228-236 | DOI: 10.32508/stdj.v18i2.1188
Published: 2015-06-30

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Copyright The Author(s) 2023. This article is published with open access by Vietnam National University, Ho Chi Minh city, Vietnam. This article is distributed under the terms of the Creative Commons Attribution License (CC-BY 4.0) which permits any use, distribution, and reproduction in any medium, provided the original author(s) and the source are credited. 

Abstract

Graphene has attracted studies because of its superior properties and potential applications. In this research, we aimed to implement a friendly environmental method to produce TiO2/graphene composite by using photo-catalyst materials – TiO2 nanotubes – to reduce graphene oxide. The TiO2 nanotubes was synthesized by alkaline hydrothermal treatment method, and have the surface area (BET) of 418,3 m2/g, and diameter of 8-10 nm. Graphene oxide with 2- 5 graphene layers was produced by Hummers method. The mixture of GO and TiO2 in water, with the ratio mTiO2/mGO = 1/1, was irradiated under an UVC-20W light during different time (1, 3, 5, 7, and 9 h). The reduction of GO to graphene was investigated by semi-quantitative infrared spectroscopy and electrical conductivity. Results showed that the reduction of GO reached to the maximum after 5 hours; and the electrical conductivity of the TiO2/ graphene composite was 0,13 S.cm-1.

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