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A new method to exfoliate Graphite oxide and application for synthesis Graphene by chemical method

Tam Thanh Mai 1, *
Nhan Thuc Chi Ha 1
Huy Thuc Ha 1
  1. University of Science, VNU-HCM
Correspondence to: Tam Thanh Mai, University of Science, VNU-HCM. Email: pvphuc@vnuhcm.edu.vn.
Volume & Issue: Vol. 17 No. 2 (2014) | Page No.: 27-34 | DOI: 10.32508/stdj.v17i2.1312
Published: 2014-06-30

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Copyright The Author(s) 2023. This article is published with open access by Vietnam National University, Ho Chi Minh city, Vietnam. This article is distributed under the terms of the Creative Commons Attribution License (CC-BY 4.0) which permits any use, distribution, and reproduction in any medium, provided the original author(s) and the source are credited. 

Abstract

A new method to separate graphite oxide (GO) modified by polyethylene oxide (PEO) by the aid of ultrasonic radiation was developed. Modified GO (graphene oxide or single layer of graphite oxide) did not show not appear crystalline peak (d002) on the X-Ray and took the form of a single layer graphene oxide on the image AFM and TEM. The exfoliated graphene oxide was reduced (RGO) to graphene by the reducing agent system HI – Acetic acid (HI-AcOH). The sheet resistance of RGOHI-AcOH is about 120 Ω/sq in the form graphene paper. In addition, FTIR, UV-Vis and Raman spectra showed more clearly about characteristics of graphite oxide, graphene oxide and RGOHI-AcOH.

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