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Preparation of polyimide from melamine and pyromellitic dianhydride by microwave irradiation

Cuong Ngoc Hoang 1, *
Vu Anh Huynh 1
  1. VNUHCM-University of Science
Correspondence to: Cuong Ngoc Hoang, VNUHCM-University of Science. Email: pvphuc@vnuhcm.edu.vn.
Volume & Issue: Vol. 19 No. 4 (2016) | Page No.: 103-112 | DOI: 10.32508/stdj.v19i4.690
Published: 2016-12-31

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Copyright The Author(s) 2023. This article is published with open access by Vietnam National University, Ho Chi Minh city, Vietnam. This article is distributed under the terms of the Creative Commons Attribution License (CC-BY 4.0) which permits any use, distribution, and reproduction in any medium, provided the original author(s) and the source are credited. 

Abstract

Under microwave irradiation, the reaction time of PMDA and melamine in DMSO was shortened to just 30 minutes. Structure of the obtained polyimide was characterized by FTIR, and its thermal stability was confirmed by TGA analysis. The longer reaction time in DMSO solution up to 30 h at high temperature was required.

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